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1 article(s) from Britner, Judita

Methylenelactide: vinyl polymerization and spatial reactivity effects

Judita Britner and
Helmut Ritter

Beilstein J. Org. Chem. 2016, 12, 2378–2389, doi:10.3762/bjoc.12.232

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Graphical Abstract

Figure 1: Structures of used monomers and the time-conversion plot of the corresponding free-radical polymeri...

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Scheme 1: Stereospecific propagation of chiral MLA illustrating the triade formation [15].

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Figure 2: Plot of log P_n versus log [In] of the polymerization of MLA with different mol % AIBN.

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Scheme 2: Postulated mechanism of the self-initiation of MLA.

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Figure 3: DFT-calculated C–C binding length (yellow) of (A) MLA and (B) the corresponding radical.

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Figure 4: IR spectra of (A) MLA and of (B) poly(MLA) prepared by the self-initiated polymerization at 70 °C.

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Figure 5: Conversion plot of the polymerization of MLA in 1,4-dioxane and DMF (c_MLA = 1.8 mol L⁻¹, c_AIBN = 1....

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Figure 6: UV–vis spectra of the reaction mixture with DPPH radical at the beginning (violet line, 0.23 mM) of...

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Figure 7: Copolymer composition curves for the systems MLA with styrene and MMA.

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Figure 8: ¹H NMR spectrum of MLA with 1 equiv of thioacetic acid and 0.15 equivalents of an inhibitor 4-metho...

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Scheme 3: Mechanism of RAFT polymerization [24].

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Figure 9: Structures of used RAFT agents examined in the polymerization of MLA.

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Figure 10: A) Kinetic plot for the RAFT copolymerization of MLA and DMA for the ratio 90/10 employing EMP. B) ...

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Published 14 Nov 2016

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